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• W2317382030 endingPage "2989" @default.
• W2317382030 startingPage "2982" @default.
• W2317382030 abstract "A series of arsenotungstates formulated as (H2en)3.5[HAs2W8O31]·6H2O (1), Na0.5(H2en)6.5{Ni3(en)[B-α-AsW9O34][B-β-AsW8O31]}Cl1.5·9H2O (2), and [H2en]4{[Ni4(Hen)2][B-α-AsW9O34]2}·5H2O (3) have been sequentially synthesized by controlling the reaction process. First, 1 was synthesized in an aqueous medium by the reaction of NiCl2 and NaAsO2 with Na2WO4, then colorless crystals of 1 transformed to yellow-green crystals of 2 for the further development of slow solvent evaporation, and, finally, yellow crystals of 3 generated over a sufficiently long time of solvent evaporation. 3 can also be hydrothermally synthesized in three different routes. Notably, 1 presents a [HAs2W8O31]7– building block, 2 exhibits an asymmetric sandwich-type arsenotungstate encapsulating two nonequivalent Keggin fragments [B-α-AsW9O34]9– and [B-β-AsW8O31]9–, and 3 is composed of two [B-α-AsW9O34]9– units sandwiching a tetranickel cluster. Their structural difference indicates that controlling the reaction process plays a key role in the structures and topologies of these complexes" @default.
• W2317382030 created "2016-06-24" @default.
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• W2317382030 date "2013-05-30" @default.
• W2317382030 modified "2023-10-18" @default.
• W2317382030 title "A Series of Arsenotungstates Based on the [HAs₂W₈O₃₁]^7– Building Block: Syntheses by Control of the Reaction Process" @default.
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• W2317382030 doi "https://doi.org/10.1021/cg4004033" @default.
• W2317382030 hasPublicationYear "2013" @default.
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