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• W2317385820 abstract "In this article, we addressed a feasible and versatile method of the fabrication of porous polyimide microspheres presenting excellent heat resistance. The preparation process consisted of two steps. Firstly, a novel polyimide/nano-silica composite microsphere was prepared via the self-assembly structures of poly(amic acid) (PAA, precursor of PI)/nanosized SiO2 blends after in situ polymerization, following the two-steps imidization. Subsequently, the encapsulated nanoparticles were etched away by hydrofluoric acid treatment, giving rise to the pores. It is found the composite structure of PI/SiO2 is a precondition of the formation of nanoporous structures, furthermore, the morphology of the resultant pore could be rela- tively tuned by changing the content and initial morphology of silica nano-particles trapped into PI matrix. The thermal properties of the synthesized PI porous spheres were studied, indicating that the introduction of nanopores could not effec- tively influence the thermal stabilities of PI microspheres. Moreover, the fabrication technique described here may be extended to other porous polymer systems." @default.
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• W2317385820 date "2015-01-01" @default.
• W2317385820 modified "2023-09-26" @default.
• W2317385820 title "Thermo-stabilized, porous polyimide microspheres prepared from nanosized SiO2 templating via in situ polymerization" @default.
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• W2317385820 doi "https://doi.org/10.3144/expresspolymlett.2015.3" @default.
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