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- W2317387532 abstract "The role of the ammonium ion during iron deposition in a ferrous sulfate bath was investigated. When cathodic polarizations were performed in a solution of 0.02 M FeSO 4 at pH 3, quartz crystal microbalance measurements showed that the presence of ammonium sulfate led to increased mass growth of Fe metal on the cathode surface. The surface pH was measured by placing a flat-bottom electrode behind a stainless steel cathode mesh. Potentiodynamic sweeps generated pH versus potential curves which revealed that in the presence of ammonium sulfate surface pH rose to alkaline levels. These two sets of findings (i.e., mass growth rate of Fe metal and surface pH results) suggest that the ammonium ion enables formation of ferrous ammine species (e.g., Fe(NH 3 ) 2 2+ and Fe(NH 3 ) 4 2+ ). This inhibits Fe(OH) 2 precipitation on the electrode, a process that can lead to surface passivation, and therefore, limited Fe metal deposition." @default.
- W2317387532 created "2016-06-24" @default.
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- W2317387532 date "2019-12-21" @default.
- W2317387532 modified "2023-09-23" @default.
- W2317387532 title "Electrodeposition of Iron in Aqueous Ferrous Sulfate Solution:Role of Ammonium Ion" @default.
- W2317387532 doi "https://doi.org/10.1149/1.2196018" @default.
- W2317387532 hasPublicationYear "2019" @default.
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