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- W2317389947 abstract "It is often necessary that gas chromatographic columns are operated at such a high temperature as the use of them which is almost limited due to the high vapor pressure of the stationary liquid phase. In such cases, the stability of the retention volumes and of the separations are impaired during an operation for a long time by the decrease of the amount of the stationary liquid phase (bleeding). In order to reduce this difficulty, the GC which connected with a pre-mixed column in front of the column as shown in Figure 1 was designed. The carrier gas was saturated with the stationary liquid phase in the pre-mixed column kept at the same temperature as the column, and was introduced into the column.The efficiency of the pre-mixed column, η, which is the ratio of changes in the retention times when the operation is conducted without and with pre-mixed column was derived theoretically as given in equation (6). The experimental results of isopropyl benzene of D. O. P. column at 160°C supported these considerations." @default.
- W2317389947 created "2016-06-24" @default.
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- W2317389947 date "1972-01-01" @default.
- W2317389947 modified "2023-09-25" @default.
- W2317389947 title "The stabilization of volatile stationary liquid phase by pre-mixed column" @default.
- W2317389947 doi "https://doi.org/10.2116/bunsekikagaku.21.12_1643" @default.
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