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• W2317505944 abstract "The reactions of sulfido-bridged dimolybdenum and ditungsten complexes [M2S2(μ2-S)2(S2CNEt2)2] (1; M = Mo, W) with an equimolar amount of [M‘Cl(PPh3)3] (M‘ = Rh, Ir) gave a series of mixed-metal incomplete cubane-type sulfido clusters [M‘(PPh3)2(μ3-S)(μ2-S)3{M(S2CNEt2)}2(μ2-Cl)]. On the other hand, mixed-metal cubane-type sulfido clusters [{M‘(cod)}2{MCl(S2CNEt2)}2(μ3-S)4] (M‘ = Rh, Ir; cod = 1,5-cyclooctadiene) were obtained by the reactions of 1 with an equimolar amount of [M‘Cl(cod)]2. Detailed structures of [Ir(PPh3)2(μ3-S)(μ2-S)3{W(S2CNEt2)}2(μ2-Cl)]·2CH2Cl2 (3b·2CH2Cl2) and [{Rh(cod)}2{MoCl(S2CNEt2)}2(μ3-S)4]·0.5CH2Cl2 (4a·0.5CH2Cl2) have been determined by X-ray crystallography. Compound 3b·2CH2Cl2 crystallized in the monoclinic system, space group P21/n, with a = 10.521(4) Å, b = 32.325(5) Å, c = 17.277(3) Å, β = 96.34(2)°, and Z = 4. Refinement by full-matrix least-squares techniques gave final residuals R = 0.071 and Rw = 0.068. Compound 4a·0.5CH2Cl2 crystallized in the monoclinic system, space group P21/c, with a = 32.900(3) Å, b = 10.847(4) Å, c = 26.312(4) Å, β = 111.274(8)°, and Z = 8. Refinement by full-matrix least-squares techniques gave final residuals R = 0.047 and Rw = 0.048." @default.
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• W2317505944 date "1998-12-10" @default.
• W2317505944 modified "2023-10-10" @default.
• W2317505944 title "Syntheses and Structures of Mixed-Metal Sulfido Clusters Containing Incomplete Cubane-Type M₂M‘S₄ and Cubane-Type M₂M‘₂S₄ Cores (M = Mo, W; M‘ = Rh, Ir)" @default.
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• W2317505944 doi "https://doi.org/10.1021/ic981035r" @default.
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