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- W2317776410 abstract "A combination of synchrotron powder X-ray diffraction (XRD) and Raman spectroscopy has been used to study high-pressure behavior of the zircon-type LaVO4 nanorods. In situ high-pressure XRD results identified an irreversible zircon-to-monazite phase transition at ∼5 GPa and a reversible transition to an undetermined second high-pressure phase (phase III) at ∼12.9 GPa. Through Le Bail refinements of the XRD patterns with zircon-type structure, we show that the zircon-type LaVO4 nanorods possess the smallest bulk modulus among zircon-type rare-earth orthovanadates. Furthermore, negative pressure coefficients of external translational T(Eg) and internal υ2(B2g) bending modes have been observed in Raman measurements. The Raman spectra of phase III with distinctive features have been fully recorded for the first time, and a related structure associated with a coordination increase for V is suggested in terms of the postmonazite phase in LaVO4 nanorods. Finally, analysis of the transmission electron microscopy both before and after compression indicates that a large number of nanorods can be recovered in the quenched samples, allowing us to verify the orientation relationship for zircon-to-monazite phase transformation." @default.
- W2317776410 created "2016-06-24" @default.
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- W2317776410 date "2015-04-06" @default.
- W2317776410 modified "2023-09-27" @default.
- W2317776410 title "Pressure-Induced Phase Transformations of Zircon-Type LaVO<sub>4</sub> Nanorods" @default.
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- W2317776410 doi "https://doi.org/10.1021/acs.jpcc.5b01007" @default.
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