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• W2317789310 abstract "The transfer of a Diels–Alder reaction of (cyclohexa-1,5-dien-1-yloxy)trimethylsilane 1 with α-acetoxyacrylonitrile 2 and acrylonitrile 8, respectively, from batch to continuous mode is presented, using standard and widely available laboratory equipment. A standard microwave-based system was used as probe for the transfer to flow reactors. Temperature and residence time have been optimized in small coiled-tube reactors and confirmed with two production runs in a flow reactor. The inherent increase in safety caused by the small volumes at high temperatures and the achieved productivity (approximately 100 g/h using acrylonitrile) are offering advantages over the batch mode which suffers from thermokinetic limitations for scale-up." @default.
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• W2317789310 date "2011-12-27" @default.
• W2317789310 modified "2023-10-01" @default.
• W2317789310 title "High-Temperature Diels–Alder Reactions: Transfer from Batch to Continuous Mode" @default.
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• W2317789310 doi "https://doi.org/10.1021/op200320w" @default.
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