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- W2317972912 abstract "A 16-hour acid-digestion procedure has been developed to prepare fish flesh or sediments for total mercury analysis. A 5-gram aliquot is treated with 10 mls. of 36 N H2SO4 and 10 mls. of 16 N HNO3. KMnO4 crystals are added with constant stirring until an excess of permanganate is achieved. The sample is then digested for 16 hours at 60?C in a water bath, maintaining a slight permanganate excess in the solution. Following digestion, the sample is cooled to ambient temperature and diluted. Total concentrations are determined by the Hatch and Ott flameless atomic absorption method. Recoveries of mercuric chloride spikes added to fish and sediment samples averaged 97.4% and 98.7%, respectively; recoveries of methyl mercuric ch!oride spikes added to fish and sediment samples averaged 95.6% and 98.7%, respectively. Trans. Kans. Acad. Sci., 76 (1), 1973." @default.
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- W2317972912 date "1973-01-01" @default.
- W2317972912 modified "2023-09-27" @default.
- W2317972912 title "Low-Temperature Digestion Method for Fish Tissue and Sediment Prior to Total Mercury Analysis" @default.
- W2317972912 doi "https://doi.org/10.2307/3627244" @default.
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- W2317972912 hasPublicationYear "1973" @default.
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