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- W2318133182 abstract "Abstract One- and two-step syntheses of 2,2′-bibenzimidazole were compared. Diethylene glycol was used as solvent that provides good solubility of the substrates. The limitation of the one-step preparation is the formation of the by-product, fluoflavine. The two-step synthesis proceeds with the separation of the intermediate product, 1,4-dihydroquinoxaline-2,3-dione, and the final product is only 2,2′-bibenzimidazole. The total yield of the two-step synthesis is above 85%." @default.
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- W2318133182 date "2014-05-12" @default.
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- W2318133182 title "The use of diethylene glycol in the synthesis of 2,2′-bibenzimidazole from <i>o</i>-phenylenediamine and oxalic acid" @default.
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- W2318133182 doi "https://doi.org/10.1515/hc-2013-0241" @default.
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