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- W2318178148 abstract "建立了凝胶渗透色谱（GPC）去脂,气相色谱-负化学电离源-质谱（GC-NCI-MS）法测定人血清中2,2’,4,4’,5,5’-六溴联苯（BB-153）、1,2-二（2,4,6-三溴苯氧基）乙烷（BTBPE）和德克隆（Dechlorane plus,DP,包括syn-DP和anti-DP）的方法。人血清样本加入内标13C12BB-153和13C10syn-DP,经蛋白质变性、脂肪提取、GPC去脂、酸性硅胶柱净化后,利用气相色谱-负化学电离源-质谱法测定样品中BB-153,BTBPE,syn-DP和anti-DP,监测离子分别为m/z 627.5,629.5,m/z 79,81以及m/z 652,654。结果表明,13 C12 BB-153和13 C10syn-DP的血清加标回收率分别为91.5%±8.9%和92.3%±8.1%,检出限为0.6～1.2 ng/g脂肪。应用本方法对人血样品进行测定,BB-153和BTBPE在所有样本中均未检出,syn-DP和anti-DP的浓度范围分别是0.7～9.2 ng/g脂肪和0.6～2.0 ng/g脂肪。" @default.
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- W2318178148 date "2013-07-24" @default.
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- W2318178148 title "Determination of New Halogenated Flame Retardants in Human Serum by Gel Permeation Chromatography Gas Chromatography-Mass Spectrometry" @default.
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