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• W2318673612 startingPage "3476" @default.
• W2318673612 abstract "Three cyclodextrine derivatives (6A,6D-di-O-(prop-2-one-1,3-dienyl)-α-cyclodextrin (1), 6-O-(prop-2-one-1-yl)-α-cyclodextrin (2) and 6A,6D-di-O-(prop-2-one-1,3-dienyl)-β-cyclodextrin (3)) were synthesised and investigated as epoxidation catalysts. The three compounds were synthesised from the corresponding perbenzylated cyclodextrins which were mono- or didebenzylated in the 6-position using Sinaÿ's method. Reaction with NaH and methallyl chloride in the case of 2, or methallyl dichloride in the case of 1 and 3, followed by dihydroxylation, periodate cleavage and protection group removal gave the target compounds. All three compounds catalysed, in the presence of oxone, the epoxidation of a series of alkenes. Epoxidation was compared to the reaction catalysed by simple ketones and inhibition was studied." @default.
• W2318673612 created "2016-06-24" @default.
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• W2318673612 date "2004-01-01" @default.
• W2318673612 modified "2023-09-25" @default.
• W2318673612 title "Cyclodextrins containing an acetone bridge. Synthesis and study as epoxidation catalysts" @default.
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• W2318673612 doi "https://doi.org/10.1039/b410098k" @default.
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