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• W2318785061 abstract "Asari Radix et Rhizoma is a herbal medicine for the treatment of common cold, rhinitis, etc. An ultra performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometry method has been established for the rapid analysis of 22 components in 27 samples from the raw materials of Asari Radix et Rhizoma and an adulterant. A total of 5 lignans, 5 essential oils, 3 aristolochic acids, 4 alkamides, and 5 flavanoids were identified by co-chromatography of samples extracts and comparison of the retention time, UV spectra, characteristic molecular ions, and fragment ions with those of authentic standards, or tentatively identified by MS/MS determination along with MassFragment software. Moreover, the method was validated for the simultaneous quantification and semi-quantification of 20 components. The samples from <i>Asarum heterotropoides</i> var. <i>mandshuricum</i> differed in the quantity of 2-methoxyl-4,5-methylenedioxypropiophenone and kakuol from those of <i>Asarum sieboldii</i> var<i>. seoulense</i>, and the chemical difference was supported by principal component analysis and orthogonal partial least squared discriminant analysis based on dataset obtained from UHPLC-QTOF/MS. In comparison with the samples from the two medicinal <i>Asarum</i> species mentioned above, those from <i>A. himalaicum</i> differed in the quality and quantity of major compounds and contained higher amounts of aristolochic acid I." @default.
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• W2318785061 date "2014-12-16" @default.
• W2318785061 modified "2023-09-24" @default.
• W2318785061 title "Simultaneous Determination of Twenty-Two Components in Asari Radix et Rhizoma by Ultra Performance Liquid Chromatography Coupled with Quadrupole Time-of-Flight Mass Spectrometry" @default.
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• W2318785061 doi "https://doi.org/10.1055/s-0034-1383296" @default.
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