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- W2318823052 abstract "Abstract Nanosized zirconium carbide (ZrC) was synthesized successfully by a novel hydrothermal precursor conversion method using chelation of polydentate glucose as the carbon source. During the pyrolysis, the core-matrix structure of intimate nanosized ZrO 2 and amorphous carbon mixture forms, resulting in short diffusion path and limit of grain growth. ZrC first appears at a much lower temperature of 1200 °C and completes conversion at 1400 °C in comparison with that of precursor without hydrothermal treatment. By raising the heating temperature to 1600 °C, oxygen content could be reduced (0.55 wt%) with a low residual carbon content (2.3 wt%), and the average size of the spherical crystallite increases from 100 nm to 200 nm. Based on above ZrC powders, the additive-free ceramic with 99.4% relative density by spark plasma sintering (SPS) at a low temperature of 1700 °C has been achieved." @default.
- W2318823052 created "2016-06-24" @default.
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- W2318823052 date "2016-07-01" @default.
- W2318823052 modified "2023-10-16" @default.
- W2318823052 title "Synthesis and pyrolysis evolution of glucose-derived hydrothermal precursor for nanosized zirconium carbide" @default.
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- W2318823052 doi "https://doi.org/10.1016/j.ceramint.2016.03.171" @default.
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