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- W2319327229 abstract "The reaction of a sulfur ylide with a chiral non-racemic sulfinyl imine afforded the desired aziridine in excellent yield and subsequent oxidation of the sulfinyl moiety dissolved in anhydrous dichloro-methane using a 75% aqueous solution of 3-chloro-per-oxy-benzoic acid afforded the title compound, C(14)H(27)NO(6)S. The configuration of the newly formed stereogenic center at the point of attachment of the 1,4-dioxane ring to the aziridine ring is S. The configurations of the pre-existing sites 2-, 5-, and 6-positions of the 1,4-dioxane ring prior to reaction of sulfinyl imine with the sulfur ylide are S, R, and R, respectively. The C-N bond lengths of the aziridine are 1.478 (2) and 1.486 (2) Å." @default.
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- W2319327229 date "2010-11-27" @default.
- W2319327229 modified "2023-10-18" @default.
- W2319327229 title "(2<i>S</i>)-2-[(2<i>S</i>*,5<i>R</i>*,6<i>R</i>*)-5,6-Dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]-1-[(<i>S</i>)-1,1-dimethylethylsulfonyl]aziridine" @default.
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- W2319327229 doi "https://doi.org/10.1107/s1600536810048816" @default.
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