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- W2319469969 abstract "Dimethyl sulfoxide (DMSO) with sodium carbonate (Na2CO3) is an effective catalyst system for C60 cyclopropanation through the Bingel reaction. Various bromomalonic esters, brominated β-keto esters, brominated 1,3-diketones, and other bromo-substituted active methylene compounds can react with C60 in the presence of DMSO and Na2CO3 to achieve excellent yields of the corresponding methanofullerenes at 10 °C. Moreover, this proposed methodology has been also employed successfully to functionalize [70]fullerene, single-walled carbon nanotubes (SWNTs), and graphene. This protocol is beneficial because it involves short reaction time, high yield, and a simple procedure. Additionally, this method does not need a strong base, such as sodium hydride and 1,8-diazabicyclo[5,4,0]undec-7-ene, because inexpensive Na2CO3 can be the catalyst." @default.
- W2319469969 created "2016-06-24" @default.
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- W2319469969 date "2015-03-09" @default.
- W2319469969 modified "2023-10-10" @default.
- W2319469969 title "DMSO: An Efficient Catalyst for the Cyclopropanation of C<sub>60,</sub> C<sub>70</sub>, SWNTs, and Graphene through the Bingel Reaction" @default.
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- W2319469969 doi "https://doi.org/10.1021/ie504918f" @default.
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