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• W2319697994 abstract "An expeditious and multikilogram-scale process for the Balz–Schiemann synthesis of o-difluorobenzene from o-fluoroaniline via two separate continuous flow reactors in 90.0% yield has been set up. The main steps involved the generation of stable diazonium fluoborate intermediate in situ via continuous diazotization reactor at 20 °C, and the choice of o-difluorobenzene as cosolvent to achieve the continuous flow fluorodediazoniation system. Reaction time of both steps could be brought down to within 10 s and 2 min, respectively, by increasing the reaction temperature and thereby taking advantage of improved mass and heat transfer of a continuous flow system." @default.
• W2319697994 created "2016-06-24" @default.
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• W2319697994 date "2012-09-14" @default.
• W2319697994 modified "2023-10-07" @default.
• W2319697994 title "A Continuous Kilogram-Scale Process for the Manufacture of <i>o</i>-Difluorobenzene" @default.
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• W2319697994 doi "https://doi.org/10.1021/op300127x" @default.
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