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- W2319971064 abstract "Artificial nickel thin films, potentially useful as magnetic materials and electrocatalysts, have been prepared by electrodeposition on noble transition metal electrodes. This study employed scanning tunneling microscopy (STM) and cyclic voltammetry to study electrodeposition of Ni on Pt(111) from 0.1 M KClO4 + 1 mM HCl + 0.06 M NiCl2. Deposition of Ni was noted at potentials more positive than its Nernst potential, as proton discharge and hydrogen evolution occurred concomitantly. Bulk deposition of Ni commenced at potentials more negative than −0.6 V (vs Ag/AgCl), where reduction of water to hydrogen was imminent. The reduction reaction of Ni2+ ion to Ni metal was a slow process under the present experimental conditions, and not all Ni deposit was removed from the Pt electrode, as indicated by irreversible changes in the voltammetric profiles. In-situ STM provided direct views of the growth process and the atomic structures of the Ni thin film. The first Ni adlayer deposited at E > −0.525 V or the under..." @default.
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- W2319971064 date "2012-09-28" @default.
- W2319971064 modified "2023-09-27" @default.
- W2319971064 title "Epitaxial Electrodeposition of Nickel on Pt(111) Electrode" @default.
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- W2319971064 doi "https://doi.org/10.1021/jp3040677" @default.
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