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- W2320008800 abstract "3,3,17,17-Diethylenedioxyandrost-5-ene was obtained by ketalisation of androstenedione, which was oxidised with PDC and t-BuOOH to form 3,3,17,17-diethylene-dioxyandrost-5-ene-7-one. Stereoselective reduction of 3,3,17,17-diethylene-dioxyandrost-5-ene-7-one by NaBH 4 in the presence of CeCl 3 .6H 2 O gave 3,3,17,17-diethylenedioxy-7β-hydroxy-androst-5-ene, which was deprotected with p-toluenesulfonic acid to gave 3,3-ethylenedioxyandrost-5-ene-7β-hydroxy and androst-4,6-dien-3,17-dione. A series of androstenedione derivatives were obtained from 3,3-ethylenedioxyandrost-5-ene-7β-hydroxy by the esterification reaction. Their structures were confirmed by MS, 1 H NMR, 13 C NMR and HRMS." @default.
- W2320008800 created "2016-06-24" @default.
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- W2320008800 date "2011-08-01" @default.
- W2320008800 modified "2023-09-26" @default.
- W2320008800 title "Synthesis of Some Novel 3,3-Ethylenedioxyandrost-7β-Acyloxy-5-Ene-17-One Derivatives as Potent Aromatase Inhibitors" @default.
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- W2320008800 doi "https://doi.org/10.3184/174751911x13129058638242" @default.
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