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• W2320211526 abstract "Reaction of a balance-like dipodal ligand 2,6-bis(pyridiyl) hexahydro-4,8-ethenopyrrolo [3,4-f]isoindole-1,3,5,7-tetrone (3-pybtd) with various Cd(II) salts afforded eight complexes, namely, [Cd2(3-pybtd)2(NO3)4(C2H5OH)2(H2O)2] (1), [Cd2(3-pybtd)2(SiF6)2(DMF)4(H2O)2](H2O)4·(DMF)2 (2), {[Cd(3-pybtd)2(H2O)4](ClO4)2}n (3), {[Cd(3-pybtd)2(OTf)2]·THF}n (4), {[Cd(3-pybtd)2(SCN)2]·(H2O)2}n (5), [Cd(3-pybtd)(OTs)2(DMF)2]n (6), [Cd(3-pybtd)2(OTs)2]n (7), and {[Cd2(3-pybtd)2Cl10/3][CdCl8/3]·(H2O)3}n (8). Complexes 1 and 2 are zero-dimensional (0D) square-like or olive-like dimeric M2L2 metallacycles, showing a pair of shape-modified molecular rectangles due to different conformations of the ligands and coordination orientation of the metal centers. Complexes 3–5 are one-dimensional (1D) looplike chains composed of olive-like M2L2 metallacycle building units as in 2, showing 0D → 1D dimension increase via ligand addition, while complex 8 is a three-dimensional (3D) framework retaining the same olive-like M2L2 metallacycle, showing 0D → 3D dimension increase via linkage of μ3-Cl bridged Cd(II) clusters. Complex 6 is a wave-like MnLn chain, possessing the same ML building units as in 1 but showing 0D → 1D dimension increase via ring-opening polymerization. Replacement of DMF molecules from the coordination sphere in 6 by the ligands resulted in a two-dimensional (2D) (4, 4) network of 7, showing 1D → 2D dimension increase from 6 via ligand addition or 1D → 2D dimension increase from 3–5 via ring-opening polymerization. Complexes 3–5 also represent a series of supramolecular isomorphs displaying anion exchange properties. Electrospray ionization mass spectrometry (ESI-MS) studies in solution suggest that the discrete and infinite structures in 1, 6, and 7 are assembled from the same monomeric ML building blocks, which crystallize in a different way to lead to structural diversification via dimerization or polymerization during the crystallization." @default.
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• W2320211526 date "2012-04-05" @default.
• W2320211526 modified "2023-10-14" @default.
• W2320211526 title "Anion Modulated Structural Diversification in the Assembly of Cd(II) Complexes Based on a Balance-like Dipodal Ligand" @default.
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• W2320211526 doi "https://doi.org/10.1021/cg300051w" @default.
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