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• W2321336906 endingPage "3428" @default.
• W2321336906 startingPage "3420" @default.
• W2321336906 abstract "The bis(substituted cyclopentadienyl)lanthanide(III) halides [{LnCpR2(μ-Cl)}2] (Ln = Pr, Nd, Sm, Dy, Tb, Y), [{LnCptt2(μ-X)}2] (X = Cl, Ln = La, Nd; X = I, Ln = Tm), and [Nd(CpR‘2SiMe2)(μ-Cl)}2] and bis(substituted cyclopentadienyl)lanthanide(II) complexes [LnCpR2(THF)2] (Ln = Sm, Eu, Yb), [YbCpt2(THF)2], [LnCptt2(THF)2] (Ln = Sm, Yb), LnCpR2 (Ln = Sm, Eu, Yb), YbCpt2, LnCptt2 (Ln = Sm, Yb), and [Yb(CpR‘2SiMe2)(THF)2] (CpR = η5-C5H4{CH(SiMe3)2}, Cpt = η5-C5H4(SiMe2But), Cptt = η5-C5H3(SiMe2But)2-1,3 and CpR‘ = η5-C5H3{CH(SiMe3)2}-3) have been synthesized from the appropriate LnCl3, TmI3, or LnI2 with the selected sodium or potassium cyclopentadienide. The complexes were characterized by 1H, 13C, 29Si, and 171Yb (for Yb(II) complexes) NMR spectroscopy, elemental analysis, and mass spectrometry. The molecular structures of [{NdCpR2(μ-Cl)}2], [{TmCptt2(μ-I)}2], and [Yb(CpR‘2SiMe2)(THF)2] have been determined by single-crystal X-ray diffraction studies. Attempts to reduce the complexes [{NdCpR2(μ-Cl)}2], [{NdCptt2(μ-Cl)}2], and [{TmCptt2(μ-I)}2] are described." @default.
• W2321336906 created "2016-06-24" @default.
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• W2321336906 creator A5001301086 @default.
• W2321336906 creator A5013786268 @default.
• W2321336906 date "2000-07-21" @default.
• W2321336906 modified "2023-10-03" @default.
• W2321336906 title "Lanthanocene Chemistry with [Cp^R]^-, [Cp^t]^-, [Cp^tt]^-, and [Cp^R^‘₂SiMe₂]²^- Ligands: Synthesis and Characterization of Bis(cyclopentadienyl)lanthanide(III) Halides and Bis(cyclopentadienyl)lanthanide(II) Complexes and Crystal Structures of [{NdCp^R₂(μ-Cl)}₂], [{TmCp^tt₂(μ-I)}₂], and [Yb(Cp^R<sup…" @default.
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• W2321336906 doi "https://doi.org/10.1021/om000305m" @default.
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