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- W2321822036 abstract "The first two complexes of the trioxodinitrate anion were prepared by reaction of Zn(bipy)Cl2·1.5H2O (1·1.5H2O) with Na2N2O3·H2O in water to produce ZnII(bipy)(H2O)(N2O3) (2) and an analogous reaction of Co(bipy)2Cl2·2.5H2O (3·2.5H2O) to produce CoII(bipy)2(N2O3) (4). Both complexes are air-sensitive and crystallize in the monoclinic space group P21/n. For 2·H2O T = 24−26 °C, Z = 4, a = 7.7595(6) Å, b = 9.4798(7) Å, c = 17.197(1) Å, β = 98.142(7)°, and V = 1252.3(2) Å3. The final residuals were R1 = 0.0452, wR2 = 0.1172, and quality-of-fit = 1.057. The final model consisted of the main structure and a minor, 4% disordered component. For 4·4H2O T = −123 °C, Z = 4, a = 9.0950(9) Å, b = 17.924(3) Å, c = 13.695(2) Å, β = 90.32(1)°, and V = 2232.5(6) Å3. The final least-squares residuals were R1 = 0.0859, wR2 = 0.1975, and quality-of-fit = 0.917. A network of hydrogen bonds involving the crystal water molecules and the coordinated trioxodinitrate anion was found in each case; in 4, a series of fused four- and eight-membered rings were found to be a dominant feature in the extended structure. The structural data and the IR spectrum indicate that the N−N bond of trioxodinitrate, 1.264(5) Å in the free anion, is longer for the coordinated anion (1.280(5) Å in 2 and 1.333(11) Å in 4)." @default.
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- W2321822036 title "Complexes of the Trioxodinitrate Anion: Synthesis and Characterization of [Zn<sup>II</sup>(bipy)(H<sub>2</sub>O)(N<sub>2</sub>O<sub>3</sub>)] and [Co<sup>II</sup>(bipy)<sub>2</sub>(N<sub>2</sub>O<sub>3</sub>)]" @default.
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- W2321822036 doi "https://doi.org/10.1021/ic961194f" @default.
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