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- W2321834743 abstract "Modifications to the Popik synthesis of aza-dibenzocyclooctyne (DIBAC) derivatives are described, which avoids tedious purifications and dramatically improves the yield. A new and analogous route to biarylazacyclooctynone (BARAC) through an amide disconnection was also attempted. The BARAC derivatives prepared were found to be unstable under the conditions employed, undergoing a known rearrangement. Finally, the synthesis of a difluoro-DIBAC derivative with a second-order rate constant intermediate between DIBAC and BARAC derivatives (0.50 M–1) is described. While more difficult to synthesize, this molecule was found to be considerably more stable than any BARAC derivatives that were prepared." @default.
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- W2321834743 date "2014-01-10" @default.
- W2321834743 modified "2023-09-27" @default.
- W2321834743 title "Scalable Synthesis of Strained Cyclooctyne Derivatives" @default.
- W2321834743 doi "https://doi.org/10.1055/s-0033-1340509" @default.
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