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- W2321853834 abstract "A set of 6α- and 6β-(hydroxy, acetoxy, and p-bromobenzoyloxy)-1, 1, 10β-trimethyl-trans-decal-2-ones was synthesized in an unequivocal manner, and the 1H-nuclear magnetic resonance (NMR) spectra, TH effect (ASIS shift on continuously changing the solvent from chloroform-d to benzene-d6), and 13C-NMR spectra of these compounds are discussed in relation to the conformations of ring A. In solution, ring A of the 6β-derivatives was shown to be more distorted (flattened) than that of 6α-derivatives. This was also true in the crystalline state as determined by X-ray analyses of their p-bromobenzoates. The TH effect was found to reflect sensitively small conformational changes in ring A." @default.
- W2321853834 created "2016-06-24" @default.
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- W2321853834 date "1981-01-01" @default.
- W2321853834 modified "2023-10-17" @default.
- W2321853834 title "4,4-Dimethyl effect (2). Syntheses, 1H- and 13C-nuclear magnetic resonance spectra, and the conformations of 6.ALPHA.- and 6.BETA.-substituted-1,1,10.BETA.-trimethyl-trans-decal-2-ones (8.ALPHA.- and 8.BETA.-substituted-4,4,10.BETA.-trimethyl-trans-decal-3-ones), models of 4,4-dimethyl-steroid- and triterpenoid-3-ketones." @default.
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- W2321853834 doi "https://doi.org/10.1248/cpb.29.3238" @default.
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