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• W2321880689 endingPage "47" @default.
• W2321880689 startingPage "42" @default.
• W2321880689 abstract "The compounds MoO2Cl2L (L = 2,2′-bipyridine (bipy) (1); 4,4′-di-tert-butyl-2,2′-bipyridine (di-tBu-bipy) (2)), [MoO2Cl2(H2O)2]·(diglyme)2 (3), MoO2Cl2 (4), MoO2(CH3)2L (L = bipy (5); di-tBu-bipy (6)), [MoO3(bipy)]n (7), {[MoO3(bipy)][MoO3(H2O)]}n (8), [Mo8O22(OH)4(di-tBu-bipy)4] (9) and MoO3 (10) were tested as phosphoester bond hydrolysis promoters in aqueous media. Sodium para-nitrophenylphosphate (pNPP) was used as a model substrate for the phosphoester bond hydrolysis reaction, which was performed at 55 °C, using D2O as solvent and 100 or 10 mol% of the chosen promoter. The progression of all the reactions was monitored by 1H NMR spectroscopy. All studied systems promote phosphoester bond hydrolysis. The best performance was obtained with MoO2Cl2L compounds (1–4) and with the inorganic–organic hybrid {[MoO3(bipy)][MoO3(H2O)]}n (8). The studied compounds originate either homogeneous or solid/liquid biphasic systems. For the biphasic systems (1, 2, 5–9), the solid phase was recovered at the end of the reaction and characterized by FT-IR spectroscopy." @default.
• W2321880689 created "2016-06-24" @default.
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• W2321880689 date "2014-06-01" @default.
• W2321880689 modified "2023-10-17" @default.
• W2321880689 title "Promotion of phosphoester hydrolysis by MoO2Cl2L (L = bipyridine derivatives, H2O, no ligand), MoO2(CH3)2L (L = bipyridine derivatives) and related inorganic–organic hybrids in aqueous media" @default.
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• W2321880689 doi "https://doi.org/10.1016/j.jorganchem.2013.12.029" @default.
• W2321880689 hasPublicationYear "2014" @default.
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