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- W2322006526 abstract "A simultaneous analytical method was developed for 9 nitrophenol pesticides and 2 aromatic nitro pesticides in drinking water by HPLC. The analytical HPLC was run on a Wakosil II 3C18AR column (4.6mm i. d. ×15cm) with a gradient formed from A: 0.1M monochloroacetic acid (pH 2.5)-MeCN-0.01M sodium butanesulfonic acid (10:30:60) and B: 0.1M monochloroacetic acid (pH 2.5)-MeCN (10:90), UV detection at 280nm and amperometric detection (AMD) with a glassy-carbon electrode (+1.2V). A drinking water sample was adjusted to pH 4 with 0.1M hydrochloric acid and purified on a Sep-pak Plus PS-2 cartridge. The cartridge was washed with water, and retained substances were eluted with MeCN. The eluate was concentrated under an N2 stream and was analyzed by HPLC. Recoveries for pesticides spiked into drinking water were 58.0-98.6% at the level of 20μg/L. The detection limits of these pesticides in water are 1μg/l." @default.
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- W2322006526 date "1996-01-01" @default.
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- W2322006526 title "Determination of Nitrophenol Pesticides in Mineral Water and Tap Water by HPLC with Ultraviolet and Amperometric Detection" @default.
- W2322006526 doi "https://doi.org/10.3358/shokueishi.37.48" @default.
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