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- W2322193972 abstract "The synthesis of dendrimer-encapsulated palladium nanoparticles with ratios of 13 and 55 metal atoms to templating dendrimer, (Pd13- and Pd55-DENs) was successfully demonstrated with the use of hydroxyl-terminated generation 4 and 5 (G4 and G5) poly(amidoamine) (PAMAM) dendrimers as both templating and stabilizing agents. These Pd-DENs catalysts were fully characterized using spectroscopic techniques. High resolution transmission electron microscopy (HRTEM) was used for the determination of particle size. The average particle sizes were found to be 1.33 ± 0.15 and 1.66 ± 0.20 nm in diameters for Pd13 and Pd55-DENs, respectively. These catalysts were evaluated using the widely utilized model reaction, 4-nitrophenol (NP) reduction by sodium borohydride (NaBH4). The experimentally determined kinetic data was modeled using the Langmuir–Hinshelwood equation which relates the apparent rate kapp, NP and BH4– adsorption constants, KNP and KBH4– respectively, the surface rate constant k, and the surface area, S. T..." @default.
- W2322193972 created "2016-06-24" @default.
- W2322193972 creator A5003270515 @default.
- W2322193972 creator A5005998089 @default.
- W2322193972 date "2014-08-19" @default.
- W2322193972 modified "2023-09-25" @default.
- W2322193972 title "Kinetic Evaluation of Dendrimer-Encapsulated Palladium Nanoparticles in the 4-Nitrophenol Reduction Reaction" @default.
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- W2322193972 doi "https://doi.org/10.1021/jp505571p" @default.
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