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• W2322277880 abstract "Dimeric thiolato-bridged Ni(II) and Pt(II) NHC complexes 2 and 4 have been synthesized from ligand precursor A through a combined and in situ deprotonation/hydrolysis protocol of a thioester-functionalized benzimidazolium salt in the presence of the respective metal salts. Reactivity studies of 2 and 4, and their previously reported Pd(II) analogue 1a toward either Me3OBF4, NaOH, or Na2S·9H2O revealed clear differences. Complex 2 decomposed when treated with Me3OBF4. On the other hand, its reaction with aqueous NaOH solution in the presence of NaBF4 yielded trinuclear [Ni3S3O] complex 6, which possesses an interesting [Ni3S3] triangle with a capping μ3-oxido ligand. Pt(II) analogue 4 was converted to the tetranuclear [Pt4S4] macrocycle 5 when treated with Me3OBF4, in analogy to the result from 1a, while no defined products could be isolated when 4 was treated with either NaOH or Na2S·9H2O. Pd(II) analogue 1a reacted with Na2S·9H2O to give the tripalladium [Pd3S3S] complex 7 bearing a capping μ3-sulfido ligand." @default.
• W2322277880 created "2016-06-24" @default.
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• W2322277880 creator A5069200805 @default.
• W2322277880 date "2013-05-16" @default.
• W2322277880 modified "2023-10-08" @default.
• W2322277880 title "A Comparative Study on Dinuclear and Multinuclear Ni(II), Pd(II), and Pt(II) Complexes of a Thiolato-Functionalized, Benzannulated <i>N</i>-Heterocyclic Carbene Ligand" @default.
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• W2322277880 doi "https://doi.org/10.1021/ic400672z" @default.
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