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• W2322283061 abstract "Autothermal reforming (ATR) has been performed over 2 wt % Ni/Ce–Zr–O/monolith catalysts in a fixed-bed reactor at atmospheric pressure with complete conversion of n-dodecane at 700 °C. The O/C ratio (0.6–1.1) was investigated. At optimal O/C ratio (0.9) the maximum H2-rich syngas yield could be achieved with both upstream (746 °C) and downstream (709 °C) monolith temperatures above 700 °C. BET surface area and Ni dispersion were measured, while temperature-programmed oxidation (TPO), temperature-programmed reduction (TPR), scanning electronic microscopy (SEM), and X-ray diffraction (XRD) were used to characterize carbon deposition and nickel status. TPO and SEM showed that carbon deposited on the monolith decreases with increasing O/C ratio and along the axial direction from upstream to downstream. The effect of catalyst calcination treatment (700 to 1200 °C) on the yields of H2, CO/CO2, and C1–C4 hydrocarbon products was also studied with ATR O/C ratios at 0.6 and 0.9. The amount of deposited carbon decreased with increasing calcination temperature and a carbon-free operation could be achieved on the 1000 °C-calcined catalyst. The high-temperature calcination resulted in the decrease of H2 yield but increased the yield of C1–C4 hydrocarbons. Quantitative H2 chemisorption and in situ TPR–TPO indicated the loss of metallic Ni due to the formation of Ni2SiO4 from the solid-state interaction of Ni and cordierite, which was confirmed by XRD of the catalysts calcined at 1200 °C." @default.
• W2322283061 created "2016-06-24" @default.
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• W2322283061 date "2015-01-09" @default.
• W2322283061 modified "2023-09-23" @default.
• W2322283061 title "Ni-Based Monolith <i>n</i>-Dodecane Reforming Catalysts: Optimization of O/C and Effect of Ni Interaction with Cordierite" @default.
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• W2322283061 doi "https://doi.org/10.1021/ie504067b" @default.
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