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- W2322372515 abstract "In this work, a novel approach to obtain high yield to poly-tert-butylglycerolethers by glycerol etherification reaction with tert-butyl alcohol (TBA) is proposed. The limit of this reaction is the production of poly-ethers, which inhibits the formation of poly-ethers potentially usable in the blend with conventional diesel for transportation. The results herein reported demonstrate that the use of a water permselective membrane offers the possibility to shift the equilibrium toward the formation of poly-ethers since the water formed during reaction is continuously and selectively removed from the reaction medium by the recirculation of the gas phase. Using a proper catalyst and optimizing the reaction conditions, in a single experiment, a total glycerol conversion can be reached with a yield to poly-ethers close to 70%, which represents data never before reached using TBA as reactant. The approach here proposed could open up new opportunities for all catalytic reactions affected by water formation." @default.
- W2322372515 created "2016-06-24" @default.
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- W2322372515 date "2014-05-09" @default.
- W2322372515 modified "2023-09-27" @default.
- W2322372515 title "Glycerol Etherification with TBA: High Yield to Poly-Ethers Using a Membrane Assisted Batch Reactor" @default.
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- W2322372515 doi "https://doi.org/10.1021/es4053413" @default.
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