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W2323736652 abstract "Photoionization mass spectrometry is a powerful method for time- and space-resolved chemical analysis of reactants, intermediates, and products. Tunable synchrotron light enables isomer separation based on unique photoionization spectra; however, mixtures of three or more isomers can be difficult to resolve by this method. In this work we demonstrate, by measuring the photoelectron spectrum corresponding to each cation m/z ratio, that imaging photoelectron photoion coincidence spectroscopy provides a more detailed spectral fingerprint than photoionization spectra. This method offers increased selectivity for analyzing gas-phase mixtures of many components. Mixtures of two C4H6 and four C5H8 unsaturated hydrocarbons were analyzed, and the components could easily be identified based on mass-selected threshold photoelectron spectra (scanning the photon energy) or photoelectron velocity map images (PEVMIs) at a single or a few fixed photon energies. The PEVMI approach is more highly multiplexed, trading somewhat lower spectral resolution for faster data acquisition and photoelectron angular distributions." @default.
W2323736652 created "2016-06-24" @default.
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W2323736652 date "2013-08-19" @default.
W2323736652 modified "2023-10-15" @default.
W2323736652 title "Mass-Resolved Isomer-Selective Chemical Analysis with Imaging Photoelectron Photoion Coincidence Spectroscopy" @default.
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W2323736652 doi "https://doi.org/10.1021/jz401500c" @default.
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