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• W2324149172 abstract "The diphosphine 4,6-bis(3-diisopropylphosphinophenyl)dibenzofuran (abbreviated as iPrDPDBFphos) was prepared and studied for its potential as a trans-chelating ligand in transition-metal coordination complexes. In the rhodium norbornadiene complex [(iPrDPDBFphos)Rh(NBD)]BF4, which has been characterized with multinuclear NMR spectroscopy, X-ray crystallography, and electrochemical studies, the ligand binds in cis fashion. In the bis(acetonitrile) complexes of rhodium and palladium [(iPrDPDBFphos)M(CH3CN)2](BF4)n (M = Rh, Pd; n = 1, 2), the ligand adopts a trans coordination geometry. Density functional theory (DFT, M06-L) calculations predict that the trans conformer is energetically more favorable than the cis by 3.5 kcal/mol. Cyclic voltammograms of the bis(acetonitrile) Pd(II) and Rh(I) complexes contain reversible and quasi-reversible reduction events, respectively, which are preliminarily assigned as metal-based redox reactions." @default.
• W2324149172 created "2016-06-24" @default.
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• W2324149172 creator A5066931781 @default.
• W2324149172 date "2011-02-17" @default.
• W2324149172 modified "2023-10-16" @default.
• W2324149172 title "Study of the Conformationally Flexible, Wide Bite-Angle Diphosphine 4,6-Bis(3-diisopropylphosphinophenyl)dibenzofuran in Rhodium(I) and Palladium(II) Coordination Complexes" @default.
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• W2324149172 doi "https://doi.org/10.1021/ic102373w" @default.
• W2324149172 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/21329367" @default.
• W2324149172 hasPublicationYear "2011" @default.
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