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• W2324153158 endingPage "4984" @default.
• W2324153158 startingPage "4973" @default.
• W2324153158 abstract "The reactions of the in situ prepared organotin(I) compounds RSnSnR with diaryl dichalcogenides ArEEAr provided, depending on the ratio of the reactants, the intramolecularly coordinated heteroleptic organotin(II) chalcogenoarylates RSnEAr (1, R = 2,6-(Me2NCH2)2C6H3, E = S, Ar = Ph; 2, R = 2,6-(Me2NCH2)2C6H3, E = Se, Ar = Ph; 3, R = 2,6-(Me2NCH2)2C6H3, E = Te, Ar = Ph; 6, R = 4-t-Bu-2,6-{P(O)(O-i-Pr)2}2C6H2, E = Se, Ar = Ph; 7, R = 4-t-Bu-2,6-{P(O)(O-i-Pr)2}2C6H2, E = Te, Ar = Ph; 8, R = 4-t-Bu-2,6-{P(O)(O-i-Pr)2}2C6H2, E = Se, Ar = 2-C5H4N) and the corresponding organotin(IV) compounds RSn(EAr)3 (4, R = 2,6-(Me2NCH2)2C6H3, E = S, Ar = Ph; 5, R = 2,6-(Me2NCH2)2C6H3, E = Se, Ar = Ph; 10, R = 4-t-Bu-2,6-{P(O)(O-i-Pr)2}2C6H2, E = S, Ar = 2-C5H4N), respectively. Compound 10 undergoes a thermally initiated cyclization reaction to give the benzoxaphosphastannole derivative {1(P),3(Sn)-Sn(S-Py)2-OP(O)(O-i-Pr)-6-t-Bu-4-P(O)(Oi-Pr)2}C6H2 (11). The compounds were characterized by 1H, 13C, 31P, 119Sn, and 125Te NMR and IR spectroscopy, electrospray ionization mass spectrometry, and single-crystal X-ray diffraction analysis. The intramolecular Sn–N and Sn–O distances range between 2.501(3) (2) and 2.815(3) Å (4) and between 2.407(2) (8·C7H8) and 2.497(2) Å, respectively. Compounds 6 and 7 show intermolecular secondary Sn···Sn interactions at distances of 3.8876(3) and 3.8379(5) Å, respectively." @default.
• W2324153158 created "2016-06-24" @default.
• W2324153158 creator A5010830762 @default.
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• W2324153158 creator A5070555642 @default.
• W2324153158 creator A5076620253 @default.
• W2324153158 creator A5087774783 @default.
• W2324153158 date "2013-08-20" @default.
• W2324153158 modified "2023-10-14" @default.
• W2324153158 title "Reactivity of Organotin(I) Dimers RSnSnR (R = 2,6-(Me₂NCH₂)₂C₆H₃, 4-<i>t</i>-Bu-2,6-{P(O)(O-<i>i</i>-Pr)₂}₂C₆H₂) with Diaryl Dichalcogenides, ArEEAr (E = S, Se, Te; Ar = Ph, 2-C₅H₄N): Control of Secondary Sn···Sn Interactions by Intramolecular Coordination and Identity of the Aryl Chalcogenate" @default.
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• W2324153158 doi "https://doi.org/10.1021/om400694z" @default.
• W2324153158 hasPublicationYear "2013" @default.
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