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• W2324283088 abstract "Hydrothermal reaction between Zn(OAc)2·2H2O and three asymmetric semirigid V-shaped multicarboxylate ligands H3L1–3 with the help of a 4,4'-bipyridine (4,4'-bpy) or 1,4-bis(imidazol-1-ylmethyl)benzene (bix) linker led to the isolation of six new coordination polymers, including [Zn3(L1)2(4,4′-bpy)2]n·(H2O)2n (1), [Zn3(L2)2(4,4′-bpy)(H2O)2]n·(H2O)2n (2), [Zn3(L3)2(4,4′-bpy)2(H2O)4]n·(H2O)6n (3), [Zn3(L1)2(bix)3]n·(H2O)7n (4), [Zn3(L2)2(bix)3]n·(H2O)4n (5), and [Zn3(HL3)2(bix)2]n (6), where H3L1, H3L2, H3L3 ligands represent 3-(2-carboxyphenoxy)phthalic acid, 4-(2-carboxyphenoxy)phthalic acid, 3-(4-carboxyphenoxy)phthalic acid, respectively. Single crystal X-ray diffraction analysis reveals a three-dimensional (3D) network for 1 and 3–5 but a two-dimensional (2D) structure for 2 and 6. Despite the construction from the polymetallic chains connected by the 4,4′-bpy ligands for both compounds 1 and 2, a 3D architecture was revealed for the former species while a 2D configuration for the latter one. Complex 3 contains open nanotube building units composed of sole 44-numbered metallomacrocycles. For 4, the 20-numbered metallomacrocycle subunits linked by Zn ions give a 1D chain, which further form a 3D polymeric structure with the help of the other cyclic-shaped subunits made from the bix ligands and Zn ions. A 3D framework of 5 is generated from the 2D sheets simplified as a (6,3) net bound by the bix ligands. Compound 6 shows a 2D corrugated framework simplified as a (4,4) net assembled by the bix ligand and dinuclear zinc unit as node. These results seem to suggest that the diversity in the building subunits formed in 1–6 actually originates from the intrinsic nature of the three asymmetric V-shaped tricarboxylate ligands together with the tunable coordination geometry and molecular configurations of ligands by the N-donor ligand employed. In addition, the thermal stability and luminescence properties for the series of six complexes have also been investigated." @default.
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• W2324283088 date "2013-09-25" @default.
• W2324283088 modified "2023-10-16" @default.
• W2324283088 title "Self-Assembled Zn(II) Coordination Complexes Based on Mixed V-Shaped Asymmetric Multicarboxylate and N-Donor Ligands" @default.
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• W2324283088 doi "https://doi.org/10.1021/cg4007372" @default.
• W2324283088 hasPublicationYear "2013" @default.
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