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• W2324339877 abstract "We report the intramolecular double compaction of sequence-controlled linear macromolecules into structured random coils. These compartmentalized single-chain objects were prepared by performing successive cross-linking reactions in an orthogonal fashion. The foldable precursors were synthesized by sequence-controlled copolymerization of styrene with N-substituted maleimides (MIs), namely pentafluorophenyl 4-maleimidobenzoate (1) and TIPS-protected N-propargyl maleimide (2). These two functional MIs allow intramolecular cross-linking. The activated ester pentafluorophenyl moieties of 1 were reacted with ethylenediamine, whereas the deprotected alkyne functions of 2 were self-reacted by Eglinton coupling. The compaction of model copolymers containing only one cross-linkable zone (i.e., either 1 or 2) was first studied. (1)H NMR and SEC analysis indicated that these structures could be efficiently compacted into single-chain objects. Thus, more complex copolymers containing two individually addressable cross-linking zones were prepared and sequentially compacted. Detailed characterization of the folding process indicated that double-compaction occurred and that the formed single-chain particles contain distinct cross-linked subdomains." @default.
• W2324339877 created "2016-06-24" @default.
• W2324339877 creator A5006612391 @default.
• W2324339877 creator A5038666668 @default.
• W2324339877 date "2014-09-09" @default.
• W2324339877 modified "2023-09-25" @default.
• W2324339877 title "Compartmentalization of Single Polymer Chains by Stepwise Intramolecular Cross-Linking of Sequence-Controlled Macromolecules" @default.
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• W2324339877 doi "https://doi.org/10.1021/ja507889x" @default.
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• W2324339877 hasPublicationYear "2014" @default.
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