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- W2324895964 abstract "Described is a new strategy using cocrystallization, one of the crystal engineering techniques, to convert a racemic compound crystal into a racemic mixed crystal which can show preferential enrichment, a symmetry-breaking spontaneous enantiomeric resolution phenomenon observed upon recrystallization of a certain kind of racemic mixed crystal with a fairly ordered arrangement of the two enantiomers under nonequilibrium conditions. The 1:1 cocrystal (2) of (dl)-phenylalanine (Phe) and fumaric acid satisfied the requirements proposed for the occurrence of preferential enrichment, such as (i) a sufficient solubility difference (racemic crystal ≪ enantiomeric crystal), (ii) the occurrence of polymorphic transition during crystallization, and (iii) the deposition of nonracemic mixed crystals with a unique crystal structure, and thus successfully showed preferential enrichment. In contrast, a racemic compound (dl)-Phe itself failed to show a polymorphic transition during crystallization and thereby preferential..." @default.
- W2324895964 created "2016-06-24" @default.
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- W2324895964 date "2011-01-05" @default.
- W2324895964 modified "2023-10-18" @default.
- W2324895964 title "Observation of Efficient Preferential Enrichment Phenomenon for a Cocrystal of (<scp>dl</scp>)-Phenylalanine and Fumaric Acid under Nonequilibrium Crystallization Conditions" @default.
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- W2324895964 doi "https://doi.org/10.1021/cg1015274" @default.
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