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- W2325285040 abstract "電気絶縁油中に微量含まれた汚染PCBのGC分析では, ECDに応答する油中成分の除去が重要である。そこで油中妨害成分の究明に油中成分をタイプ別に分離し, ECDへの寄与を比較した結果, 極性成分, 多環および2環芳香族成分の寄与が大きいことが明らかになった。これらの成分の除去にはフロリシル/シリカゲル2層吸着クロマトグラフィーが有効かつ迅速であった。本前処理法でのPCB回収率は85±5%, 検出下限はパックドカラムを用いた場合で0.1μg/g, キャピラリーカラムを用いた場合で0.01μg/gが確認された。" @default.
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- W2325285040 date "1991-01-01" @default.
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- W2325285040 title "Clean-up procedure to remove interfering substances for the determination of trace levels of polychrorinated biphenyls in electrical insulating oils." @default.
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- W2325285040 doi "https://doi.org/10.1627/jpi1958.34.191" @default.
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