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• W2325468729 abstract "This study presents a new synthetic method for fabricating yolk@shell-structured barium magnesium silicate (BMS) particles through a template-engaged solid-state reaction. First, as the core template, (BaMg)CO3 spherical particles were prepared based on the coprecipitation of Ba(2+) and Mg(2+) . These core particles were then uniformly shelled with silica (SiO2 ) by using CTAB as the structure-directing template to form (BaMg)CO3 @SiO2 particles with a core@shell structure. The (BaMg)CO3 @SiO2 particles were then converted to yolk@shell barium magnesium silicate (BMS) particles by an interfacial solid-state reaction between the (BaMg)CO3 (core) and the SiO2 (shell) at 750 °C. During this interfacial solid-state reaction, Kirkendall diffusion contributed to the formation of yolk@shell BMS particles. Thus, the synthetic temperature for the (BaMg)SiO4 :Eu(3+) phosphor is significantly reduced from 1200 °C with the conventional method to 750 °C with the proposed method. In addition, the photoluminescence intensity of the yolk@shell (BaMg)SiO4 :Eu(3+) phosphor was found to be 9.8 times higher than that of the conventional (BaMg)SiO4 :Eu(3+) phosphor. The higher absorption of excitation light by the structure of the yolk@shell phosphor is induced by multiple light-reflection and -scattering events in the interstitial void between the yolk and the shell. When preparing the yolk@shell (BaMg)SiO4 :Eu(3+) phosphor, a hydrogen environment for the solid-state reaction results in higher photoluminescence efficiency than nitrogen and air environments. The proposed synthetic method can be easily extended to the synthesis of other yolk@shell multicomponent metal silicates." @default.
• W2325468729 created "2016-06-24" @default.
• W2325468729 creator A5018593047 @default.
• W2325468729 creator A5050540359 @default.
• W2325468729 date "2016-04-05" @default.
• W2325468729 modified "2023-10-16" @default.
• W2325468729 title "Template-Engaged Solid-State Synthesis of Barium Magnesium Silicate Yolk@Shell Particles and Their High Photoluminescence Efficiency" @default.
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• W2325468729 doi "https://doi.org/10.1002/chem.201504528" @default.
• W2325468729 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/27059894" @default.
• W2325468729 hasPublicationYear "2016" @default.
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