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- W2325519918 abstract "Abstract The one-dimensionally disordered structure of the composite crystal of synthetic (LaS) 1.18 VS 2 has been determined based on the X-ray diffraction intensities collected by using monochromatized synchrotron radiation of wavelength 1.180 Å. The ordered (100) projection was refined based on 94 unique intensities collected on a diffractometer using Mo K α radiation; R = 0.067, R w = 0.084. The structure consists of interleaved layers of LaS and VS 2 , each of them forming a substructure which can be described based on a C -centred orthorhombic lattice with a 1 = 5.705(1) Å, b = 5.828(1) Å, c = 22.32(2) Å and Z = 8 for LaS and a 2 = 3.366(3) Å, b = 5.828(1) Å, c = 22.32(2) Å and Z = 4 for VS 2 . The b and c axes are common to both substructures. D x = 4.806 Mg m −3 . The structure of the (100) projection is isotypic with that of the orthorhombic (PbS) 1.18 TiS 2 ; plane group pgm , b ′ = b /2, c ′ = c . The La and S atoms of LaS are arranged like Na and Cl in the NaCl structure. The V atom is surrounded by six S atoms octahedrally. The LaS layers are related to each other through a twofold screw axis parallel to [100] with a screw translation of ±0.32 a 1 , while the nearest VS 2 layers are coupled by a glide plane perpendicular to [001] with a glide translation of ±0.25 a 2 . Stochastic change of the signs causes a one-dimensional disorder." @default.
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- W2325519918 date "1995-06-01" @default.
- W2325519918 modified "2023-09-25" @default.
- W2325519918 title "Struktur des eindimensional fehlgeordneten Kompositkristalls (LaS)1,18VS2" @default.
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- W2325519918 doi "https://doi.org/10.1524/zkri.1995.210.6.432" @default.
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