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- W2326451736 abstract "Three new polymorphs of C60·2S8 were discovered. The previously known structure (first reported by Roth and Adelmann in 1993 hereby designated as α) crystallizes in space group C2/c with Z = 4 and changes to a triclinic structure (β) in space group P1̅ with Z = 4 when the temperature is decreased below 260 K. The room-temperature structure was reinvestigated, and the new, ordered, low-temperature structure is described. A new, concomitant, polymorph (γ) crystallizes in space group P21/c with Z = 4 at room temperature and undergoes a phase change to Pc (δ) with Z = 4 when the temperature is decreased below 180 K. As indicated by geometric and temperature factor changes, it is clear that the low-temperature phases represent an increase in the level of order in the arrangement of C60 molecules. Both of the phase changes are reversible." @default.
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- W2326451736 date "2014-11-21" @default.
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- W2326451736 title "New Insights into the Structural Complexity of C<sub>60</sub>·2S<sub>8</sub>: Two Crystal Morphologies, Two Phase Changes, Four Polymorphs" @default.
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- W2326451736 doi "https://doi.org/10.1021/cg501486x" @default.
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