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- W2326647777 abstract "Borole systems tend to undergo various reactions driven by the disruption of its destabilizing antiaromatic character. As a consequence, the isolation and characterization of free boroles is challenging, especially when the substituents around the C4B framework are sterically less demanding. In the present paper we report the synthesis of 1-bromo-2,3,4,5-tetraphenylborole. The title compound readily undergoes a dimerization/rearrangement reaction in analogy to the previously reported 1-chloro-2,3,4,5-tetraphenyborole to form an isostructural product identified by X-ray crystallography. Additionally we present the formation of Lewis acid–base adducts of the title compound with 3,5-lutidine, PCy3, N-hetrocyclic carbene, cyclic (amino)(alkyl)carbene, and THF. The latter compounds were analyzed by single-crystal X-ray diffraction and compared." @default.
- W2326647777 created "2016-06-24" @default.
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- W2326647777 date "2011-05-10" @default.
- W2326647777 modified "2023-10-01" @default.
- W2326647777 title "Unwinding Antiaromaticity in 1-Bromo-2,3,4,5-tetraphenylborole" @default.
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- W2326647777 doi "https://doi.org/10.1021/om200315p" @default.
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