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- W2327139780 abstract "Indium–tin oxide (ITO) nanoparticles, 6.1 ± 0.8 nm in diameter, were synthesized using a hot injection method. After reaction with 3-aminopropyldimethylethoxysilane to replace the initial oleylamine and oleic acid capping ligands, the aminated nanoparticles were rendered electroactive by functionalization with ferrocenoyl chloride. The nanoparticle color changed from blue-green to light brown, and the nanoparticles became more soluble in polar solvents, notably acetonitrile. The nanoparticle diffusion coefficient (D = 1.0 × 10–6 cm2/s) and effective ferrocene concentration (C = 0.60 mM) in acetonitrile solutions were determined using ratios of DC and D1/2C data measured by microdisk voltammetry and chronoamperometry. The D result compares favorably to an Einstein–Stokes estimate (2.1 × 10–6 cm2/s), assuming an 8 nm hydrodynamic diameter in acetonitrile (6 nm for the ITO core plus 2 nm for the ligand shell). The ferrocene concentration result is lower than anticipated (ca. 1.60 mM) based on a potentiometric titration of the ferrocene sites with Cu(II) in acetonitrile. Cyclic voltammetric data indicate tendency of the ferrocenated nanoparticles to adsorb on the Pt working electrode." @default.
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- W2327139780 date "2012-12-26" @default.
- W2327139780 modified "2023-10-10" @default.
- W2327139780 title "Synthesis and Electrochemistry of 6 nm Ferrocenated Indium–Tin Oxide Nanoparticles" @default.
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- W2327139780 doi "https://doi.org/10.1021/la304443k" @default.
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