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• W2327266552 abstract "Novel A-site ordered perovskites CaPd(3)Ti(4)O(12) and CaPd(3)V(4)O(12) were synthesized under high-pressure and high-temperature of 15 GPa and 1000 °C. These compounds are the first example in which a crystallographic site in a perovskite-type structure is occupied by Pd(2+) ions with a 4d(8) low spin configuration. The ionic models for these compounds were determined to be Ca(2+)Pd(2+)(3)Ti(4+)(4)O(12) and Ca(2+)Pd(2+)(3)V(4+)(4)O(12) by structural refinement using synchrotron X-ray powder diffraction, hard X-ray photoemission, and soft X-ray absorption spectroscopy. Magnetic susceptibility, electrical resistivity, and specific heat measurements demonstrated diamagnetic insulating behavior for CaPd(3)Ti(4)O(12) in contrast to the Pauli-paramagnetic metallic nature of CaPd(3)V(4)O(12)." @default.
• W2327266552 created "2016-06-24" @default.
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• W2327266552 date "2013-01-18" @default.
• W2327266552 modified "2023-10-02" @default.
• W2327266552 title "Pd²⁺-Incorporated Perovskite CaPd₃<i>B</i>₄O₁₂ (<i>B</i> = Ti, V)" @default.
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• W2327266552 doi "https://doi.org/10.1021/ic3025155" @default.
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