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• W2327458488 abstract "An efficient synthesis of boronated phosphines with an o-phenylene-bridge prepared from sec-phosphine boranes and using benzyne chemistry is reported. Successive reactions of sec-phosphine boranes with n-BuLi and 1,2-dibromobenzene, and then with boron reagents, afford the o-boronatophenylphosphine derivatives in 71% yields. The use of P-chirogenic sec-phosphine boranes leads to the free boronated phosphines with retention of configuration at the P-center after decomplexation. The reaction of P-chirogenic o-boronatophenylphosphine with KHF2 affords the corresponding trifluoroborated phosphine with ee >98%." @default.
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• W2327458488 date "2015-02-13" @default.
• W2327458488 modified "2023-09-29" @default.
• W2327458488 title "Efficient Synthesis of (P-Chirogenic) <i>o</i>-Boronated Phosphines from <i>sec</i>-Phosphine Boranes" @default.
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• W2327458488 doi "https://doi.org/10.1021/acs.orglett.5b00167" @default.
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