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• W2328601014 abstract "A homochiral helical three-dimensional coordination polymer, poly[[(μ 2 -acetato-κ 3 O , O ′: O )(hydroxido-κ O )(μ 4 -5-nicotinamido-1 H -1,2,3,4-tetrazol-1-ido-κ 5 N 1 , O : N 2 : N 4 : N 5 )(μ 3 -5-nicotinamido-1 H -1,2,3,4-tetrazol-1-ido-κ 4 N 1 , O : N 2 : N 4 : N 5 )dicadmium(II)] 0.75-hydrate], {[Cd 2 (C 7 H 5 N 6 O) 2 (CH 3 COO)(OH)]·0.75H 2 O} n , was synthesized by the reaction of cadmium acetate, N -(1 H -tetrazol-5-yl)isonicotinamide (H-NTIA), ethanol and H 2 O under hydrothermal conditions. The asymmetric unit contains two crystallographically independent Cd II cations, two deprotonated 5-nicotinamido-1 H -1,2,3,4-tetrazol-1-ide (NTIA − ) ligands, one acetate anion, one hydroxide anion and three independent partially occupied water sites. The two Cd II cations, with six-coordinated octahedral and seven-coordinated pentagonal bipyramidal geometries are located on general sites. The tetrazole group of one symmetry-independent NTIA − ligand links one of the independent Cd II cations into 6 1 helical chains, while the other NTIA − ligand links the other independent Cd II cations into similar but unequal 6 1 helical chains. These chains, with a pitch of 24.937 (5) Å, intertwine into a double-stranded helix. Each of the double-stranded 6 1 helices is further connected to six adjacent helical chains through an acetate μ 2 -O atom and the tetrazole group of the NTIA − ligand into a three-dimensional framework. The helical channel is occupied by the isonicotinamide groups of NTIA − ligands and two helices are connected to each other through the pyridine N and carbonyl O atoms of isonicotinamide groups. In addition, N—H...O and O—H...N hydrogen bonds exist in the complex." @default.
• W2328601014 created "2016-06-24" @default.
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• W2328601014 date "2015-03-14" @default.
• W2328601014 modified "2023-09-30" @default.
• W2328601014 title "A three-dimensional cadmium(II) coordination polymer with unequal homochiral double-stranded concentric helical chains" @default.
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• W2328601014 doi "https://doi.org/10.1107/s2053229615004258" @default.
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