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- W2329071456 abstract "chloro-2-oxo-butyric acid ethyl ester 5 is an important intermediate in many biologically active compounds such as thiazole carboxylic acids. In this work, a rapid synthetic method for compound 5 was established. The compound 5 was synthesized from the commercially available diethyl oxalate through two steps including nucleophilic substitution, chlorinated. The structure was confirmed by MS and 1 HNMR. Furthermore, the synthetic method was optimized. The total yield of the two steps was30%" @default.
- W2329071456 created "2016-06-24" @default.
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- W2329071456 date "2016-01-01" @default.
- W2329071456 modified "2023-09-24" @default.
- W2329071456 title "Synthesis of 3-chloro-2-oxo-butanoate" @default.
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- W2329071456 doi "https://doi.org/10.2991/icmmct-16.2016.150" @default.
- W2329071456 hasPublicationYear "2016" @default.
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