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• W2329139639 endingPage "845" @default.
• W2329139639 startingPage "836" @default.
• W2329139639 abstract "Wet chemistry-based techniques, including widely used hydrothermal and solvothermal synthesis, have emerged as thriving strategies for nanostructure bulk synthesis, which in reality encountered the ubiquitous challenge of corrosion problems during scale-up or further commercialization. In this contribution, as an endeavor, uniform and pore-free Mg2B2O5 nanowhiskers with a length of 120–3000 nm, a diameter of 40–160 nm, and an aspect ratio of 2–34 were successfully synthesized via a novel, green, noncorrosive, easy scale-up hydrothermal–thermal conversion route. Specifically, the NaCl byproduct of the room-temperature coprecipitation system was preseparated by filtration, and then the cake was transferred for hydrothermal conversion to avoid the corrosion of Cl–, giving rise to uniform MgBO2(OH) nanowhiskers. The MgBO2(OH) nanowhiskers were calcined for high crystallinity Mg2B2O5 nanowhiskers, assisted by NP-9 and preseparated byproduct NaCl. The present novel hydrothermal synthetic route to MgBO2(OH) nanowhiskers was carried out at 200 °C (40 °C lower than previous work), definitely indicating green characteristics, such as energy savings, reduction and reuse of byproduct, noncorrosiveness to hydrothermal apparatus, and easy scale-up. The as-developed strategy provided a feasible and operable solution to the bottleneck of the hydrothermal scale-up of MgBO2(OH)/Mg2B2O5 nanowhiskers. Not only was this enlightening for mass production of other nanostructures, especially for the chlorate-participated system in academia and industry, but this also could contribute to sustainable development of our society." @default.
• W2329139639 created "2016-06-24" @default.
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• W2329139639 date "2014-02-04" @default.
• W2329139639 modified "2023-10-02" @default.
• W2329139639 title "Green, Noncorrosive, Easy Scale-Up Hydrothermal–Thermal Conversion: A Feasible Solution to Mass Production of Magnesium Borate Nanowhiskers" @default.
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• W2329139639 doi "https://doi.org/10.1021/sc400481j" @default.
• W2329139639 hasPublicationYear "2014" @default.
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