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- W2329452009 abstract "A fluorometric method for the determination o 1-(2-o-chlorobenzoyl-4-chlorophenyl)-5-glycylaminomethyl-3-dimethylaminocarbonyl-1H-1, 2, 4-triazole hydrochloride dihydrate (1) was established. This highly sensitive method was applied to the analysis of animal feed spiked with the drug. Compound 1 was easily transformed into the fluorophore 4-amino-7-chloro-5-(o-chlorophenyl)-[1, 2, 4]triazolo[1, 5-a]quinoline-2-carboxylic acid (2) in alkaline solution. After the extraction of 1 from the feed, 1 was converted into 2. The strong fluorescence of 2 allowed the establishment of a method with a quantitation limit of 5 mg/kg.Compound 1 in feed samples spiked at 10-500mg/kg was determined with a coefficient of variation of less than 10%. The concentration of 1, its uniformity in the whole feed and its stability can be evaluated by this method." @default.
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- W2329452009 date "1986-01-01" @default.
- W2329452009 modified "2023-10-16" @default.
- W2329452009 title "Analytical studies on 1-(2-o-chlorobenzoyl-4-chlorophenyl)-5-glycylaminomethyl-3-dimethylaminocarbonyl-1H-1,2,4-triazole hydrochloride dihydrate. II. A fluorometric method applicable to animal feed." @default.
- W2329452009 cites W1607104652 @default.
- W2329452009 doi "https://doi.org/10.1248/cpb.34.2873" @default.
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