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• W2330000858 endingPage "1297" @default.
• W2330000858 startingPage "1294" @default.
• W2330000858 abstract "A concise synthesis of the dihydro-α-pyrone/dihydro-γ-pyrone natural product (+)-obolactone (13) is disclosed. The dienediol acetonide 23 (≥97% ee) was obtained from 1,5-dichloropentane-2,4-dione in four steps. A Wacker monooxidation of 23 furnished the monoketone 24 in 64% yield. The OH group of the ensuing dihydro-γ-pyrone 31 was esterified under Mitsunobu conditions with cinnamic acid (→ 80% inversion and 20% retention of configuration). A ring-closing metathesis formed the dihydro-α-pyrone moiety of the target in the terminating step." @default.
• W2330000858 created "2016-06-24" @default.
• W2330000858 creator A5032839055 @default.
• W2330000858 creator A5088592033 @default.
• W2330000858 date "2013-03-01" @default.
• W2330000858 modified "2023-10-15" @default.
• W2330000858 title "Enantioselective Synthesis of (+)-Obolactone Based on a Symmetry-Breaking Wacker Monooxidation of a Diene" @default.
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• W2330000858 doi "https://doi.org/10.1021/ol400232m" @default.
• W2330000858 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23451721" @default.
• W2330000858 hasPublicationYear "2013" @default.
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