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- W2330328085 abstract "By reaction of Na2[B9H9] with the appropriate N-halogenosuccinimide, the monohalogenated anion [1-XB9H8]2- (X = Cl, Br, or I) is formed. The X-ray diffraction analyses performed on single crystals of (Ph4P)2[1-XB9H8].CH3CN (X = Cl, Br, I) reveal that the tricapped trigonal prismatic geometry of the cluster is retained after substitution in the 1-position. Crystallographic data are as follows for (Ph4P)2[1-XB9H8].CH3CN. X = Cl, Br: monoclinic, space group P2(1), a = 10.7 A, b = 32.9 A, c = 13.8 A, beta = 96 degrees, Z = 4, R1 = 0.038 and R1 = 0.036, respectively. X = I: monoclinic, space group P2(1)/n, a = 10.5 A, b = 13.6 A, c = 33.4 A, beta = 94 degrees, Z = 4, R1 = 0.094. The compounds have been characterized by vibrational and 11B NMR spectroscopy as well." @default.
- W2330328085 created "2016-06-24" @default.
- W2330328085 creator A5008576559 @default.
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- W2330328085 date "2000-06-28" @default.
- W2330328085 modified "2023-10-16" @default.
- W2330328085 title "Synthesis of Monohalogeno Derivatives of <i>closo</i>-[B<sub>9</sub>H<sub>9</sub>]<sup>2-</sup>. Crystal Structures of (Ph<sub>4</sub>P)<sub>2</sub>[1-XB<sub>9</sub>H<sub>8</sub>]·CH<sub>3</sub>CN (X = Cl, Br, I)" @default.
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- W2330328085 doi "https://doi.org/10.1021/ic9913334" @default.
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