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- W2330455002 abstract "D-マンニトールを原料にグリセリン誘導体である, (S) -グリセロール-1, 2-アセトニドを経て, キラルな (R) , (S) -エピクロルヒドリンを合成し, 三フッ化ホウ素工一テラートを開始剤とするカチオンオリゴメリゼーションを行った. 溶媒としてベンゼン, 1, 2-ジクロロエタンおよび1, 2-ジメトキシエタンを用いて検討した. 生成したオリゴマーについてはGPC分析により分子量分布を調べた. その結果, 溶媒により収率および分子量分布への影響がかなり異なる結果が得られた. 非極性溶媒では, 4～8量体の分布を示し, 転化率は高いが多量体への分布が多く, 1, 2-ジメトキシエタンでは, 2～6量体の分布であった. また, 開始剤濃度による収率に与える差も顕著であり, 15～87%と幅があった." @default.
- W2330455002 created "2016-06-24" @default.
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- W2330455002 date "1993-01-01" @default.
- W2330455002 modified "2023-09-25" @default.
- W2330455002 title "Synthesis of Chiral Epichlorohydrin Monomers and Effects of Monomer Chirality, Solvent, and Initiator Concentration on the Oligomerization." @default.
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